Topic : Development of Synchrotron X-ray Fluorescence system for quantitative measurements of trace elements in solid and liquid
Scope
The expeditious growth of modern industry as well as the exacerbate human activities leave various harmful residues into environment, which consequently leads to serious pollutions. Understanding, screening, and fast detection of elemental compositions, and trace heavy metal contaminations in such environmental samples would be beneficial to avoid the widespread distribution and later solve the problems. In addition, the existance of trace elements in materials could alter their physicochemical properties and emerge novel characteristic features of materials aiming for such specific applications. X-ray fluorescence (XRF) spectroscopy is one of the potential techniques for characterization of elemental compositions. XRF requires less sample preparation and can be applied for various types of samples including solid, liquid, and slurry. In addition, XRF provides availability for fast screening and database for quality and quantity control.
This project aims to develop the apparatus for XRF experiments to quantify the concentrations of elements in materials. The participants will involve in the design of the automatic sample measurement system, for example a motorized multi-sample holder, a vacuum sample chamber, a user-friendly Labview-based program for the automatic data collection. The participants will join the beamline scientists to test the XRF measurement system, perform experiments, and do quantitative XRF analysis using fundamental parameter (FP) method. Over the course of the project, the participants will independently engage in a synchrotron development similar to that of beamline scientists and will have a good understanding of beamline instrumentation, control system, and XRF data analysis.
Supervisor
Dr. Supagorn Rugmai
and SLRI researchers
Topic for Ph.D. Thesis by SLRI
1.Development of synchrotron-based advanced measurement techniques
2.Development of AI for atomic and molecular structural analyses with X-Ray Diffraction and X-ray Scattering
3.Development of X-ray lenses for nano-beam
4.Studies of collective bunch instabilities in electron storage rings
5.Studies of longitudinal dynamics of Landau cavity in electron storage ring
6.Studies of low-emittance beam injection efficiency of 4th generation synchrotron light source
7.Development of advanced photon detectors
8.Development of pulse magnets for high energy electron synchrotron
9.Development of ultra-high stability power supply
10.Advanced control system with unified classical, modern, and AI-based approaches
11.Development of Radio Frequency amplifier system
12.Development of Low Level Radio Frequency system
13.Autonomous control for Radio Frequency control system
14.Design and fabrication of Radio Frequency harmonic cavity for electron storage ring
15.Development of RF-shield bellow for low impedance electron storage ring
16.Development of high field gradient accelerating structure for industrial applications
17.Development of sub-micron resolution Synchrotron X-ray Tomography system
18.Development of Synchrotron X-ray Fluorescence system for quantitative measurements of trace elements in solid and liquid
19.Development of high field in-vacuum permanent magnet wiggler for high intensity hard x-ray generation